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http://localhost:8080/xmlui/handle/123456789/785| Title: | Reactions of MoCl5 and MoO2Cl2 with 4-Phenylimidazole- 2-thiol and 2-Thiazoline-2-thiol |
| Authors: | Rani, D Singh, G Sharma, S |
| Keywords: | FTIR; 1H NMR and LC-MS fragments MoO2Cl2; 4-Phenylimidazole-2-Thio 2-Thiazoline-2-Thiol |
| Issue Date: | 2020 |
| Publisher: | Oriental Journal of Chemistry 36 |
| Series/Report no.: | ;1096-1102. |
| Abstract: | Reactions of MoCl5/MoO2Cl2 with 4-phenylimidazole-2-thiol/2-thiazoline-2-thiol in CH3CNsolvent in 1:1/1:2 molar ratios have been carried out at room temperature. Products obtained MoCl3(C9H7N2S)(CH3CN), [1];MoCl2(C9H7N2S)(CH3CN), [2]; Mo2OCl4(C9H8N2S)2, [3] and Mo4O2Cl12(C9H7N2S)4, [4]; MoO2Cl3(C3H5NS2)2, [5] and Mo2O4Cl3(C3H5NS2)2, [6] have been analyzed and characterizedby elemental analysis, FTIR, 1H NMR and LC-MS techniques. Compounds being moisture and air sensitive, these have been prepared in inert atmosphere using vacuum line and liquid nitrogen cooled traps. Fragments obtained in LC-MS spectra support the formulae derived. |
| URI: | http://dx.doi.org/10.13005/ojc/360611 http://localhost:8080/xmlui/handle/123456789/785 |
| ISSN: | 2231-5039 |
| Appears in Collections: | Research Papers |
Files in This Item:
| File | Description | Size | Format | |
|---|---|---|---|---|
| Kindly contact to the Central Library.docx | 11.36 kB | Microsoft Word XML | View/Open |
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